INVESTIGATION OF THE EFFECT OF THERMAL TREATMENT OF A 0.4 % CARBON STEEL QUENCHED IN CASSAVA STARCH

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ABSTRACT

The possibility of using cassava liquid extracts agitated condition as quenching media for plain

carbon steel has been investigated. Agitated liquid extract from cassava were used in fresh and

fermented condition for hardening 0.35% C plain carbon steel. The mechanical properties of the

quenched samples and the cooling rate curves were used to determine the quench severity. The

microstructures of the quenched samples were also examined. Steel samples quenched in agitated cassava liquid extract showed an improvement in their mechanical properties. The

cooling rate curve shows that the fermented cassava liquid extract has a higher cooling rate

compared to oil but lower than water. The microstructure of the samples quenched in the cassava

liquid extract revealed the formation of martensite. Hence the cassava liquid extracts can be

used as quenchant in hardening process steels.

CHAPTER ONE

  1. INTRODUCTION

Quenching is a crucial process within the broader field of heat treatment. It constitutes an

important manufacturing technology in nearly every market sector. These include: railway,

automotive, aerospace and others. Quenching is used to induce hardness in steel so that it may

perform as required in service [1]. It involves heating steel to some temperature above the upper

critical temperature, in order to convert it partially or completely to austenite, holding it long

enough to ensure the desire austenization, after which cooling is carried out at a rate equal to or

faster than the critical cooling rate[2]. The two primary functions of a liquid quenchant is to

facilitate the hardening of steel by controlling heat transfer during quenching and also to

minimize the formation of undesirable thermal and transformation gradients which may lead to

increase in distortion and cracking[3].

The commonly used quenchants are water, oil, brine, and synthetic solutions. Water though

abundant and low cost has the drawback of inducing crack or dimensional changes on the

quenched component due to its high cooling rate and oil has the problem of not inducing enough

hardness. Polymer quenchant, though it can provide severity between those of water and oil, has

the problem of varying concentration during the quenching process and it is also more expensive.

Brine produces more quenching severity than water; it also has a problem of corrosive attack on

the components and the equipment used for the quenching[4-5].

The technical challenge of quenching that has since been known is the choice of a

quenching medium that will yield the desired as-quenched properties, such as hardness with

minimum induced distortion. There is need therefore for the development of a quenching

medium with good economics like water, but having less severity of quench and yet producing appreciable hardening. This work is aimed at investigating the suitability of using cassava liquid

extract in agitated condition as a quenching medium for hardening steels.

A rough estimate of about IOmill ion tonnes of cassava is processed into garri annually in

igeria alone[6]. With the ongoing aggressive and positive campaign by the igerian

government to popularize the cultivation of cassava by Nigerian farmers, and also the

introduction of improved cassava varieties by the International Institute of Tropical Agriculture,

lIT A, Ibadan, Nigeria there may be further increase in the country’s annual cassava production.

During the traditional processing of cassava starch storage root for garri production in Africa,

the fermented liquid juice squeezed off from the mesh, which is normally discarded as waste,

and do constitute environmental or health hazard. Therefore, there is need to take advantage of

this abundance and availability of cassava, sustain the development, and stop wastage of the

extract by harnessing its economic value. Steel is an alloy of iron and carbon, where other elements are present in quantities too small to affect the properties.